Three-Column Train Divided-Wall Column Side-Draw Control

Amines Separation

Commercial flowsheet for aniline, cyclohexylamine (CHA), and dicyclohexylamine (DCHA): two conventional columns for aniline and CHA, followed by a divided-wall column (DWC) with a controlled side-draw to produce high-purity DCHA.

2025
Commissioned
≥ 99.7%
CHA purity
≥ 99.8%
DCHA purity
Amines separation column system

Flowsheet Overview

  • Column 1 — Aniline: Recovery and purification.
  • Column 2 — CHA: Cyclohexylamine product column.
  • Column 3 — DWC: Divided-wall column with side-draw for DCHA; internal partition reduces remixing and improves energy use.

Performance

  • CHA ≥ 99.7 wt.% (typ.)
  • DCHA ≥ 99.8 wt.% (typ.)
  • Robust start-up and turndown; straightforward train integration